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DC Field | Value | Language |
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dc.contributor.author | Shetty, A.Nityananda | |
dc.contributor.author | Gadag, R.V. | |
dc.contributor.author | Gajendragad, M.R. | |
dc.date.accessioned | 2020-03-31T08:18:53Z | - |
dc.date.available | 2020-03-31T08:18:53Z | - |
dc.date.issued | 1989 | |
dc.identifier.citation | Indian Journal of Technology, 1989, Vol.27, 4, pp.224-226 | en_US |
dc.identifier.uri | http://idr.nitk.ac.in/jspui/handle/123456789/10299 | - |
dc.description.abstract | A method is proposed for selective complexometric determination of Pd(II) using hydroxylamine hydrochloride as a replacing (masking) agent. An excess of EDTA is added to Pd(II) solution containing associated diverse metal ions and the uncomplexed EDTA is titrated at pH 5-6 (acetic acid - acetate buffer) with lead nitrate solution using xylenol orange as indicator. Hydroxylamine hydrochloride is then added to displace EDTA from the Pd-EDTA complex. The released EDTA is titrated with standard lead nitrate solution. Reproducible and accurate results are obtained in the concentration range 0.3-15 mg of Pd with a relative error of 0.4% and coefficient of variation (n=6) not exceeding 0.4%. | en_US |
dc.title | Complexometric determination of palladium (II) using hydroxylamine hydrochloride as releasing agent | en_US |
dc.type | Article | en_US |
Appears in Collections: | 1. Journal Articles |
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